[HN Gopher] Efficient recovery and recycling of cobalt from spen...
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       Efficient recovery and recycling of cobalt from spent lithium-ion
       batteries
        
       Author : Jimmc414
       Score  : 125 points
       Date   : 2024-02-25 16:33 UTC (6 hours ago)
        
 (HTM) web link (pubs.acs.org)
 (TXT) w3m dump (pubs.acs.org)
        
       | gardenfelder wrote:
       | Clickbait? The link does not take us to a document of that title;
       | the term "urine" is nowhere to be found there.
        
         | Jimmc414 wrote:
         | This article illustrates where the term "urine" came from, but
         | to avoid the appearance of clickbait I removed the word from
         | the title.
         | 
         | https://www.thecooldown.com/green-tech/ev-battery-recycling-...
         | 
         | It would have been more accurate to say "using ingredients
         | commonly found in urine", but that is more words that can be
         | used in an HN title even though that is the entire point of the
         | post.
        
       | tgtweak wrote:
       | I don't really get the impression that current recycling
       | techniques are lacking... typically the battery packs are
       | immersion-shred and separated into the metal, plastic and the
       | cathode "paste" which is a mix of lithium, mangagnese, nickel and
       | cobalt. The recovery from there is pretty high - up to 95%.
       | 
       | The percentage of cobalt in modern lithium ion batteries (ie:
       | tesla/panasonic's nmc-811 cells) is only 8% of the battery
       | material. It's almost entirely Nickel now (72%) with traces of
       | manganese (8%) and cobalt (9%). Even the lithium percentage is
       | down to ~11%.
       | 
       | I was under the impression that the biggest issue right now was
       | scaling up recycling facilities and recycling pathways back to
       | those facilities so that they can handle the huge influx of
       | batteries anticipated in the next 3-4 years. I don't think
       | recovering 97% vs 95% of 8% of the material is going to change
       | the economics of battery recyling.
       | 
       | The more interesting breakthroughs seem to be low-temperature,
       | safe-chemical extraction. Let's not forget the advancements in
       | cell composition that will lead to longer lifespans (2-3x higher
       | cycle counts) - which not only reduces the waste from battery
       | packs but also that from devices that use them.
        
         | vinni2 wrote:
         | > I don't think recovering 97% vs 95% of 8% of the material is
         | going to change the economics of battery recyling.
         | 
         | Not yet but as more and more EVs reach end of life and these
         | rare earth metals become rarer then it starts make a
         | difference.
        
           | pfdietz wrote:
           | Neither nickel nor cobalt are rare earth metals. They may be
           | somewhat rare, and they come from the earth, but that's not
           | what "rare earth" means.
        
             | tgtweak wrote:
             | at $28,000/MT it's rare enough to worry about - for context
             | it looks like a model 3 has about 4.5KG of cobalt in it's
             | entire pack, or around ~$130 at current spot rate.
        
               | pfdietz wrote:
               | Totally irrelevant to the point I was making.
        
             | ajross wrote:
             | This is like arguing with an astronomer about what a
             | "metal" is. The colloquial definition of "rare earth
             | element" when talking about industry and not chemistry
             | generally means anything you mine that isn't an already-
             | concentrated ore.
        
               | malfist wrote:
               | What do you mean? Any element heavier than hydrogen is a
               | metal, everyone knows this.
        
               | whycome wrote:
               | Sometimes hydrogen might be a metal....
               | 
               | https://en.m.wikipedia.org/wiki/Metallic_hydrogen
        
               | pfdietz wrote:
               | Q: How many legs does a dog have, if we call a tail a
               | leg?
               | 
               | A: Four. Calling a tail a leg doesn't make it one.
               | 
               | One sometimes sees the nonsense you are describing there
               | in attempts to smear PV as dirty because it "uses rare
               | earth elements", with a pointer toward dirty REE
               | processing in China. PV does not use the actual REEs;
               | this smear exploits the terminological slovenliness being
               | engaged in here.
               | 
               | I don't believe any honest person in industry would use
               | "rare earth element" to refer to nickel or cobalt.
        
               | ajross wrote:
               | > I don't believe any honest person in industry
               | 
               | The question should be whether you were genuinely
               | confused about what the upthread commenter meant by using
               | "these rare earth metals" to refer to battery reactants.
               | You were not. You were just being a pedant. Now you're
               | heaping onto the mistake by (1) calling the upthread
               | comment "nonsense", (2) calling me "dishonest", (3)
               | calling the discussion a "smear", and "slovenly".
               | 
               | Good grief. Can you really just not? There are ways to
               | have this discussion without flinging poo...
        
               | pfdietz wrote:
               | I'm being pedantic because the confusion has been
               | exploited by bad actors in the way I described. Now, I
               | correct it, to prevent the exploit.
               | 
               | "Slovenly" is a precise description of the problem here,
               | up to and including the moral component of that word.
               | "Smear" is also accurate in what I was referring to
               | there: these were clear bad faith attempts to disseminate
               | a falsehood about PV. Your own use was not called a
               | smear, you may just be the kind of useful fool the smear
               | depended on.
        
             | justinclift wrote:
             | As additional info: https://en.wikipedia.org/wiki/Rare-
             | earth_element#Minerals
        
         | keenmaster wrote:
         | Don't underestimate the elasticity of supply.
        
           | piyh wrote:
           | We've been trying to figure out cobalt supply for a long time
           | and the DRC is still 70% of the worlds supply
           | 
           | https://www.cobaltinstitute.org/wp-
           | content/uploads/2021/06/P...
        
         | praseodym wrote:
         | The price for cobalt is currently around 30 USD/kg but has been
         | as high as 90 USD/kg:
         | http://www.dailymetalprice.com/metalpricecharts.php?c=co&u=k...
         | 
         | I'm not very familiar with the ellconomics of recycling, but I
         | doubt that this process to recover an additional 2% will be
         | cost effective.
        
           | tgtweak wrote:
           | I guess if you're a massive recycling facility and working on
           | 30,000+MT of raw batteries as input, the 2% extra could
           | equate to a fair amount, certainly when the spot price is
           | $28,000/MT.
           | 
           | Considering spot prices for cobalt are dropping quickly and
           | are now back to pre-2019 levels... not sure it makes sense to
           | invest heavily in this.
        
             | fbdab103 wrote:
             | What happens with the slag from these operations? I assume
             | it is easy enough to separate out the metals from plastics,
             | all of the metal is still potentially available for
             | reprocessing.
             | 
             | Do they keep a huge deposit of these tailings hoping for it
             | to be profitable some day?
        
         | parineum wrote:
         | > I don't think recovering 97% vs 95% of 8% of the material is
         | going to change the economics of battery recyling.
         | 
         | I think you're focusing on the wrong part of the headline.
         | 
         | > ... with common chemicals.
         | 
         | Seems much more important to the economics than, as you said,
         | the slight uptick in recovery.
        
           | NotSammyHagar wrote:
           | All of this progress is also good information to counter the
           | endless claims that electric vehicles are destroying the
           | world. There is an impact from all mining exercises and there
           | are terrible conditions in some cobalt mines. Tesla
           | apparently buys from only certified cobalt suppliers, for
           | example. But every article that talks about improvements in
           | efficiency in recycling and the continuing improvements help
           | to set the record straight.
           | 
           | We could reach almost steady state of battery materials
           | eventually with more and better battery recycling. I wonder
           | when that might be expected? 30 years for EVs to go through
           | the car fleet and replace all other cars, then most battery
           | materials can come from recycling? However there will likely
           | be different minerals in new battery tech over time, will
           | solid state batteries be as recyclable?
        
             | pompino wrote:
             | Improving public transportation is a far superior solution
             | than forcing people to buy EV cars by outlawing gas
             | engines. For the median income in the US, or person working
             | minimum wage - all of this is pie-in-the-sky elite talk.
             | EVs are essentially for rick folks to feel better about
             | themselves.
        
               | dkjaudyeqooe wrote:
               | Class warfare aside, public transport will transition to
               | EVs as well and there is a lot of promise in self driving
               | vehicles smaller than a bus making public transport
               | cheaper, more flexible, and more attractive.
               | 
               | In the end people will buy EVs because they are cheaper
               | and better. Governments are just trying to set goals and
               | promote action against climate change.
        
               | pompino wrote:
               | There is no benefit to public transport when EV companies
               | gets our tax money to build their charger network, or
               | offering thousands of dollars of tax credit to rich folks
               | to buy EVs.
               | 
               | >In the end people will buy EVs because they are cheaper
               | and better.
               | 
               | I'm hoping people switch from EVs to public transit.
               | Personally, I'm more interested in how the government can
               | expand public transit in general so that the need for EV
               | cars is eliminated or substantially reduced in the first
               | place.
        
               | dkjaudyeqooe wrote:
               | The easiest way to get people to switch to public
               | transport is to make it suck less. Short of forcing
               | people to use it that's kind of the only way. It also
               | contributes to CO2 emissions so it has to go electric and
               | improvements in EVs also helps there.
               | 
               | I can see your preference for public transport, but it's
               | already heavily subsidised and only used by a minority of
               | people in most places. Subsidies for EVs, which aim to
               | reduce emissions from cars, which are extremely popular,
               | seems quite equitable.
               | 
               | I don't think further subsidy of public transport is
               | going to materially increase its use, it has to improve
               | beyond incremental availability. As I said automated
               | vehicles are a much more promising avenue for drastically
               | increasing public transport use.
        
               | cyberax wrote:
               | Public transit is NEVER a good solution. It's at most a
               | miserable workaround for inability to use personal cars.
        
           | Animats wrote:
           | The really important point: "Furthermore, the ni-DESs are
           | highly soluble in water and can be recovered and recycled."
           | 
           | Most leaching processes produce toxic waste, often very large
           | quantities of toxic waste. It's usually soluble in water, so
           | plants have big leachate ponds, where the water evaporates,
           | leaving behind some kind of sludge. The question here is, can
           | this new leachate really be recycled effectively, or is there
           | a sludge-disposal problem?
           | 
           | This is probably a solveable problem, because recycling
           | batteries starts with a very rich resource. It's processes
           | which extract from low-grade ores that yield giant dumps of
           | leftover crud. Gold and rare earth extraction are notorious
           | for this.
        
             | lazide wrote:
             | The original mining process almost certainly involved some
             | kind of leachate processing process too. And it's pretty
             | unlikely to be worse doing it on battery components where
             | all the original components were highly refined.
        
         | tonetegeatinst wrote:
         | This is what my understanding of EV battery recycling is at. It
         | all gets shredded and then the separate the enclosure from the
         | actual battery.
         | 
         | Then they get a mixture of the annode and cathode + any
         | electrolyte solution.
         | 
         | My understanding is that the anode and cathode are separated
         | into separate containers....and who knows what the electrolyte
         | solution is doing....its probably stuck in both piles or burnt
         | off
        
         | jillesvangurp wrote:
         | > The percentage of cobalt in modern lithium ion batteries (ie:
         | tesla/panasonic's nmc-811 cells) is only 8% of the battery
         | material
         | 
         | Worth pointing out that with LFP batteries, it's actually zero
         | percent. There are a few more cobalt free battery chemistries.
         | But this is so far the most popular one with a rapidly growing
         | market share that is closing in on 40% of the market. Lots of
         | Teslas and other vehicles use them. There are a few more cobalt
         | free battery chemistries of course. Sodium ion is getting some
         | usage in China lately and does not involve cobalt, for example.
         | And some of the solid state batteries don't use it either.
         | 
         | Cobalt isn't actually controversial because it's rare but
         | because the way some of it is mined in Congo (i.e. with
         | children). Most of it is actually fine and mined in a more
         | humane way. Using children is not a hard requirement. And as
         | the article points out recycling it is pretty doable too. And
         | it's not all that rare either. It's by no means a rare earth.
         | 
         | And never mind about the other things children mine. Like
         | copper, coal, diamonds, gold, etc. Or the fact that a lot of
         | cobalt is also used in other industries. Like the oil refining
         | industry, for example. Cobalt is somehow only controversial in
         | the context of batteries. Any other form of cobalt usage is
         | apparently not worth reporting on, scrutinizing, etc.
         | 
         | A lot of crocodile tears get shed over the poor children in the
         | Congo. But only when it concerns batteries for EVs. I wonder
         | why that is (rhetorical question with some obvious answers, I
         | know) and whether those people actually really care. Because
         | they sure are being awfully selective with their outrage.
        
           | thebruce87m wrote:
           | The people who care about cobalt being used for EVs don't
           | seem to mind when you point out it's also used to refine
           | petroleum. It was never about the cobalt.
        
             | rbut wrote:
             | It would have been nice to provide a source to back up this
             | argument. So I looked it up.
             | 
             | 4% of global cobalt use is used by refineries. 62% of
             | global cobalt use is for EVs, and growing.
             | 
             | [1] https://www.perplexity.ai/search/How-much-
             | cobalt-5scBTFEHRym...
             | 
             | [2] https://www.perplexity.ai/search/How-much-
             | cobalt-5scBTFEHRym...
        
           | Jimmc414 wrote:
           | >A lot of crocodile tears get shed over the poor children in
           | the Congo. But only when it concerns batteries for EVs. I
           | wonder why that is (rhetorical question with some obvious
           | answers, I know) and whether those people actually really
           | care. Because they sure are being awfully selective with
           | their outrage.
           | 
           | Seems a bit complex for an issue as simple as you can extract
           | cobalt from spent batteries literally with human pee and
           | white vinegar as a solvent.
        
             | Turskarama wrote:
             | The point being made is that talking about the use of
             | cobalt in batteries is actually beside the point. Unless we
             | do something about child labor _in general_ then reducing
             | cobalt use will just see those children being exploited in
             | some other way. The focus on child labor for mining cobalt
             | is 100% just an attack on BEVs, it was never about the
             | children who were just being used in yet another way to
             | achieve someone elses ends.
        
         | grecy wrote:
         | > _I don 't really get the impression that current recycling
         | techniques are lacking_
         | 
         | Big money is trying as hard as possible to convince people not
         | to buy EVs, and "The batteries are not recyclable" is just
         | another wonky arrow in their bent quiver of fear, uncertainty
         | and doubt.
         | 
         | In fact, there are huge EV battery recycling plants in the US,
         | operating right now:
         | 
         | https://www.canarymedia.com/articles/recycling-renewables/th...
        
       | superkuh wrote:
       | Here's the article mirror for anyone like me getting blocked by
       | cloudflare no matter what buttons pressed or captchas solved:
       | https://web.archive.org/web/20240223190753/https://pubs.acs....
       | 
       | BTW, the N-methylurea used in this is extremely mutagenic in
       | humans.
        
         | pfdietz wrote:
         | Are you confusing that with N-nitroso-N-methylurea?
        
       | overstay8930 wrote:
       | There's no breakthrough until a business plan exists to resell
       | for a profit, otherwise it's as recyclable as plastic.
        
         | sojournerc wrote:
         | You don't think there is a market for recovered cobalt? I see
         | your point regarding recyling, but plastic just isn't as
         | valuable as cobalt, given the relative difficulty of
         | extraction.
        
           | overstay8930 wrote:
           | Of course there's a market for it, but if you can't sell it
           | for a profit then it doesn't matter how much of a
           | breakthrough your recycling project is.
           | 
           | Plastic is trivial to recycle but it's cheaper to buy new
           | plastic than to buy recycled plastic.
        
       | StarterPro wrote:
       | If only we could find a child-slavery free way to extract and
       | process the cobalt.
        
         | thebruce87m wrote:
         | There are LFP batteries that don't use cobalt if you want to
         | use less of it. It's used for refining crude oil so you can't
         | get away from it completely.
        
       | krmblg wrote:
       | Disclaimer: didn't read the paper and only have a very basic
       | understanding of chemistry (and sorry for simplifying a complex
       | topic), but started wondering whether we should be able to
       | discover useful reactions via pure calculation by now (ignoring
       | quantum effects)?
       | 
       | Despite being a specific domain, wouldn't reasoning about
       | reactions (and their efficiency in an industrial, large-scale
       | setting) be something that "models" should be able to do quite
       | "easily" (given the fact that bonding forces, energy requirements
       | and catalytic effects are sort of well-known, i.e. just some more
       | dimensions to deal with)?
        
         | spenczar5 wrote:
         | Yes, but its not easy. The devil is in the details.
         | 
         | https://en.m.wikipedia.org/wiki/Computational_chemistry
        
         | philipkglass wrote:
         | The only kind of bonds we can model reasonably well while
         | ignoring quantum effects are hydrogen bonds. Hydrogen bonds can
         | be modeled as parameterized effects in Newtonian mechanics, and
         | molecular dynamics simulations using Newtonian mechanics can
         | reproduce some interesting properties of molecules in solution.
         | 
         | The vast majority of chemical reactions involve changes in
         | electronic configuration that are only described by quantum
         | mechanics. The most accurate algorithmic approximations of
         | electron quantum mechanics have terrible scaling properties -
         | O(N^7) or worse. Due to that terrible scaling, the largest
         | high-accuracy calculations that are tractable now are not
         | _that_ much larger than those that could be completed in the
         | 1990s, despite much greater processing power.
         | 
         | There are other ways of approximating quantum effects in
         | chemistry that scale better, but they all have tradeoffs and
         | weaknesses of their own. They can used in limited domains or
         | used to guide experimental design, but they're not accurate
         | enough to discover useful reactions via pure calculation. They
         | need to work in tandem with experimental validation and it
         | requires domain experts in both the experimental and
         | theoretical work. The methods are not simple enough for a bench
         | chemist to use them as a black box for reaction discovery.
        
           | krmblg wrote:
           | Thanks for the reply, really didn't know such a vast amount
           | of chemical reactions and outcomes was grounded in QM.
        
             | mkesper wrote:
             | Probably because our school atom model is too simple.
             | https://www.quantamagazine.org/inside-the-proton-the-most-
             | co...
        
         | jabl wrote:
         | Broadly speaking, "computational materials science" has been a
         | thing for quite a while, and has been responsible for the
         | majority of academic supercomputer time allocations for
         | decades.
        
         | barbarr wrote:
         | Yes, there are many research groups working on this at the
         | moment. We can (roughly) screen through chemical reactions
         | performed in vaccuum. Even this is difficult since you either
         | need to simulate atoms bouncing around until you observe a
         | reaction (extremely slow to perform) [0], or you need to
         | numerically search for a viable reaction pathway (still quite
         | slow to perform) [1]. The main problem is that the best methods
         | scale badly with the number of atoms you're simulating, so you
         | need to trade off accuracy for speed by using less-accurate
         | methods.
         | 
         | Screening through reactions in the real world is particularly
         | hard, since you not only need to worry about the inaccuracy of
         | your simulation method, but you also need to take
         | solvent/environment effects into account. You need to trade off
         | even more accuracy for speed if you want to do so. As computing
         | power advances, there will be less pressure to make these
         | tradeoffs, but a lot of work in comp chem at the moment is
         | focused on either exploring or expanding the speed-accuracy
         | frontier.
         | 
         | [0] https://en.wikipedia.org/wiki/Transition_path_sampling
         | 
         | [1]
         | https://people.chem.ucsb.edu/kahn/kalju/chem126/public/qm_ts...
         | 
         | [2]
         | https://en.wikipedia.org/wiki/Ab_initio_quantum_chemistry_me...
        
           | krmblg wrote:
           | Thanks for the reply and the links. Really have to read up a
           | little.
        
         | lumb63 wrote:
         | Not a chemist, but I think trying to do chemistry without
         | modeling quantum effects is like trying to do physics without
         | math. The latter is necessary to express the former.
        
           | krmblg wrote:
           | Yeah, reading the sibling comments made me aware that my
           | mental model when it comes to chemistry (and the role QM
           | plays even in "simple" scenarios) needs an update.
           | 
           | Thanks for the angle!
        
       | doctorhandshake wrote:
       | As is often the case, there's a good Volts about the economics
       | (and chemistry / physics) of battery recycling:
       | 
       | https://www.volts.wtf/p/electrifying-battery-recycling
        
         | falserum wrote:
         | > it effectively replaces fire and chemicals with clean, cheap
         | renewable electricity
         | 
         | Does it mean it can work on intermittent electricity? (Cheapest
         | renewable is intermittent)
        
       | baseline-shift wrote:
       | The energy use is the issue because fossil fuels supply the heat
       | for the thermochemistry (like with most industrial processes).
       | But direct solar heat could be used instead - this heat is
       | supplied by concentrated solar thermal in a novel process
       | 
       | https://www.solarpaces.org/solar-pyrolysis-to-recycle-lithiu...
        
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