[HN Gopher] Experiments in Making Cocktail Ice
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       Experiments in Making Cocktail Ice
        
       Author : mhb
       Score  : 159 points
       Date   : 2023-05-16 13:04 UTC (9 hours ago)
        
 (HTM) web link (www.alcademics.com)
 (TXT) w3m dump (www.alcademics.com)
        
       | foobarbecue wrote:
       | When I was working on an ice climbing robot we spent a lot of
       | effort trying to get large blocks of clear ice to test on. The
       | thought was that we wanted repeatable experiments. But then we
       | realized that perfectly dense water ice is so hard and tough that
       | our robot would not be able to get an ice screw into it. So we
       | ended up trying to make something more similar to glacial ice. To
       | do that we bought a nugget ice machine, filled large aluminum
       | bins of that, and then backfilled with water, and had the robot
       | climb on those in a walk-in freezer.
       | 
       | https://eos.org/articles/meet-iceworm-nasas-new-ice-climbing...
        
         | aardvarkr wrote:
         | That's incredibly cool, thanks for sharing it!
        
       | classified wrote:
       | Cocktail ice should be formed like a duck, swimming on the
       | beverage.
        
         | psd1 wrote:
         | I had a very expensive old-fashioned once where the bartender
         | chiseled a sphere of ice out of a block. It took about five
         | minutes. The diameter was about 8cm or so.
         | 
         | He created a very spherical sphere. I twizzled it round and
         | round but could not detect any eccentricity. Clearance in the
         | tumbler was even at all orientations.
         | 
         | A carved duck might be more immediately impressive, but the
         | sphere did blow my mind.
         | 
         | It was a very good old-fashioned. I nursed it for 20 minutes -
         | it didn't get watery, as they usually do.
        
           | isleyaardvark wrote:
           | Spheres have less surface area which reduce the watering down
           | of the drink.
           | 
           | Edit: though I would bet that's less of a factor than the
           | initial temperature of the ice and the liquor.
        
       | leblancfg wrote:
       | Former bartender here. Having nice cocktail ice chunks at home
       | isn't as complex as this might make it seem. No need for a clunky
       | box in your freezer or costly gizmos.
       | 
       | I keep a travel-sized coffee thermos in my freezer with about 2-3
       | inches of water at the bottom. Takes 18-24 hours to create one
       | chunk. If you time it right, 90% of the water freezes, and the
       | water impurities pool at the bottom - pop out the frozen chunk
       | and the result is clear ice. I store 4-5 of these in a zip-top
       | bag until I have friends over and serve drinks.
       | 
       | Best to use a thermos with a slight conical interior so it's easy
       | to pop out the ice. Makes a nice plug-shaped, clear ice chunk.
       | Then refill and restart the process.
        
         | zygy wrote:
         | Have a particular one to recommend?
        
           | leblancfg wrote:
           | Whatever's cheap and slightly conical - most will do. Worst
           | case you let it sit for ~1h so it melts a little.
           | 
           | From 10 seconds of Googling, something like this:
           | https://browzefactory.com/products/tumbler-stainless-
           | steel-2...
        
         | Jarmsy wrote:
         | An even lower equipment option I've had some success with: Just
         | use any food container, such as an ice-cream box or tupperware.
         | Part fill it and put in the freezer with no lid. It will start
         | freezing from the outside in. When it is partly frozen but
         | before it goes cloudy, break a hole in the top of the ice to
         | allow the trapped liquid inside to escape, and put it back in
         | for a few more hours until it is nearly all frozen. This way
         | you can get a big mostly clear block with a cloudy bit in the
         | middle (you can repeat the break and freeze to get it even
         | smaller), which you can cut up and melt off any cloudy bits
         | with warm water.
        
         | TrainedMonkey wrote:
         | Water expands when it freezes, in my head thermos is an
         | extremely rigid structure, how do you stop it from rapturing?
        
           | account42 wrote:
           | I'm not sure if your end of the world planning needs to
           | include your thermos.
        
           | leblancfg wrote:
           | Not an issue. It's only partially filled, less than half-way.
           | As it forms, the ice floats and glides up the sides until
           | it's like, 1mm higher than where it started.
        
           | GordonS wrote:
           | Simply don't fill it to the brim, allowing room for
           | expansion.
        
           | a_t48 wrote:
           | The thermos is mostly full of compressible air
        
           | angry_moose wrote:
           | Only if its completely full. A travel thermos is ~6 inches
           | deep and OP said to fill it to 2-3 inches.
        
           | tecleandor wrote:
           | I think the idea is leaving it open so it freezes from the
           | top down. From what I've read there, the trick of clear ice
           | is directional freezing.
           | 
           | I've seen some other ideas like freezing water in a camping
           | cooler with its top open.
        
             | vladvasiliu wrote:
             | That's what I thought the idea was, too.
             | 
             | But then, why aren't my ice-cubes made in the regular
             | fridge tray clear? The same principle should apply: they
             | should be clear at the top, where the tray is open.
        
               | hollasch wrote:
               | Ice in a tray freezes from all sides since it's not
               | insulated. And indeed, the ice from your tray is crystal
               | clear on the sides, with the cloudy ice at the center of
               | the cube.
               | 
               | In an insulated vessel, the sides and bottom remain
               | liquid until the frozen portion grows down from the top,
               | pushing the cloudy bit to the bottom, which you can then
               | just lop off.
        
               | wrs wrote:
               | The thermos wall is an insulator, unlike the tray.
        
           | Swizec wrote:
           | > how do you stop it from rapturing?
           | 
           | From the post you're replying to: _2 to 3 inches of water at
           | the bottom_ ... _expands to fill the thermos_
           | 
           | Air compresses. A lot.
        
           | burnished wrote:
           | Well you make sure it isnt baptized.
           | 
           | But also as the ice freezes I believe it becomes more buoyant
           | and that rigidity causes the ice to be lifted up when it
           | exerts force on the thermos interior.
        
             | fluxic wrote:
             | Pun of the year.
        
         | boringg wrote:
         | Will be trying this. Thanks for the tip!
        
         | dabluecaboose wrote:
         | >If you time it right, 90% of the water freezes, and the water
         | impurities pool at the bottom
         | 
         | And even if you don't, worst case you end up with a cloudy end
         | on your clear ice that can be easily removed by rubbing it on
         | an aluminum sheet pan
        
           | eutectic wrote:
           | I'm not sure it will be so easy to get the ice out if you let
           | it freeze solid.
        
             | anamexis wrote:
             | Well luckily there's an easy solution for that as well:
             | letting it sit for awhile.
        
           | leblancfg wrote:
           | Or just passing the cloudy bit under hot water. Melts like a
           | charm.
        
       | jansan wrote:
       | In one method he uses a silicone mold to make a clear ice ball.
       | Note that these molds are also available for making four, six and
       | 25 ice balls, so this may be a more efficient method than it
       | looks, and no wire should be required.
        
       | kualto wrote:
       | I always thought the key to getting clear ice was to boil the
       | water first so the oxygen goes out of solution.
        
         | jcampbell1 wrote:
         | That isn't the issue. The problem is an ice shell initially
         | forms, then the water inside the shell needs to expand as it
         | freezes but it has no where to expand. This creates internal
         | stress and micro fractures and the resulting ice crackles due
         | to internal stress. Clear ice requires a directional freeze.
        
         | foobarbecue wrote:
         | You might mean air, not oxygen. Air is mostly nitrogen. Water
         | ice is 1/3rd oxygen atoms (or about 8/9ths by mass).
         | 
         | Thinking more, molecular oxygen, O2, dissolved in water is a
         | thing and it does have better solubility than nitrogen so maybe
         | you did mean molecular oxygen.
         | 
         | And yeah, we tried that, putting water in a vacuum chamber and
         | pumping out the dissolved air. It didn't seem to make much
         | difference.
        
         | samwillis wrote:
         | Interestingly freezing hot or boiled water can be quicker due
         | to the Mpemba effect.
         | 
         | https://en.wikipedia.org/wiki/Mpemba_effect
        
           | kevinmchugh wrote:
           | Faster freezing is bad when you're trying to make clear ice.
           | It's also bad to put hot water in your freezer - you're
           | bringing the temperature of everything else up and then it
           | has to refreeze. That'll damage the quality of whatever food
           | is in the freezer.
        
         | brenns10 wrote:
         | This site has whole sections on "things that don't work" and
         | "things that work, but not that well" based on experiments.
         | Here's boiling water first:
         | 
         | https://www.alcademics.com/2017/10/boiled-versus-rested-wate...
         | 
         | (Works somewhat, but not well enough)
        
         | leblancfg wrote:
         | Doesn't really work - the real trick is to make sure your ice
         | is crystallizing directionally. The impurities are the last to
         | crystallize, so this pushes them out.
         | 
         | Then you take your ice out of the container when it's 90% done,
         | and your ice chunk is clear.
        
       | alokedesai wrote:
       | I've been making clear ice at home for a while--it's a great
       | party trick and much easier to do than it seems.
       | 
       | The best part is chiseling ice cubes from a large clear block of
       | ice: use a serrated knife and a hammer and you will end up with
       | perfectly square blocks of ice.
        
         | boringg wrote:
         | Interesting trick!
        
       | burnished wrote:
       | Excellent work! I think it was this person that launched my own
       | home ice making journey.
       | 
       | My process is simple and involves freezing in quart containers
       | and then carving with a steak knife and rubber mallet. Watching
       | the freezing process has been neat, at one point I get a shell
       | that could be used as a glass by itself.
       | 
       | This might be covered by the literature but my observation is
       | that the ice becomes cloudy late in the freezing process which
       | makes me suspect the issue is small fractures or imperfections in
       | the crystal as a consequence of mechanical forces - the ice tried
       | to occupy an area that is just a touch too small. This doesn't
       | gel with other folks observations however who see cloudyness
       | before the ice fully finishes freezing.
        
       | joncrocks wrote:
       | In case anyone wants an easy way to make nice, clear ice fairly
       | easy in a home setting.
       | 
       | https://www.wintersmiths.com/ - These guys make gadgets that you
       | can put in your freezer and get very clear ice. Melt very
       | well/evenly.
       | 
       | You can also find details of their latest machine on kickstarter,
       | which is a work in progress.
       | 
       | edit: I have bought most of their products over the years,
       | starting with their first ice-baller. And supported the phantom
       | kickstarter, and their latest one.
        
       | shermablanca wrote:
       | I've purchased this one[1] and it makes almost perfect cubes of
       | ice that are very clear and melt evenly and slowly. In my
       | cocktail glass it is so flat that the whiskey does not permeate
       | the bottom. The result is a beautifully clear square in the
       | center of my glass when looking at it from above.
       | 
       | Trick is to let the ice temper for a few minutes to acclimate to
       | the room temperature before pouring your drink over it. Otherwise
       | it will crack. Also good to spin it a few times in your glass to
       | melt it a bit to get it perfectly flat.
       | 
       | [1] ClearlyFrozen High Capacity (10 x 2 Inch) Home Clear Ice Cube
       | Tray/Ice Cube Maker https://a.co/d/2E7YcmC
        
         | mastax wrote:
         | The margins on that must be incredible. An ice cube tray plus
         | some foam packing material, for $40. Didn't even bother to
         | encase the foam in a blow-molded shell like a cooler.
        
         | bertronic wrote:
         | I use this product too, love it!
        
       | vrglvrglvrgl wrote:
       | [dead]
        
       | samwillis wrote:
       | Somewhat related interesting fact, the UK ice market is dominated
       | by one player who has brought out almost all other manufacturers,
       | The Ice Co.
       | 
       | This is a good article from a couple of years ago about them:
       | https://www.theguardian.com/news/2020/dec/10/super-cubes-ins...
       | 
       | They have created a few "innovative" products, such as larger
       | "clearer" ice cubes for cocktails - related to TFA - by spraying
       | water into super cooled upside-down moulds.
        
         | yojo wrote:
         | Sounds like similar tech to the Kold-Draft machines in the US
         | market.[1] During the height of the pandemic one of my
         | neighborhood bars was selling bags of their cubes to stay
         | afloat. Only good thing to come out of covid.
         | 
         | 1: https://kold-draft.com/pages/why-kold-draft#technology
        
       | rini17 wrote:
       | Someone gonna come up with Czochralski process for
       | monocrystalline ice :)
        
       | maherbeg wrote:
       | I also recommend storing your specialty ice in a brown paper bag.
       | It'll keep for a surprisingly long while without sticking to each
       | other!
       | 
       | I have a premade directional ice kit and make 10 ice cubes per
       | night and then throw them into the paper bags. We never run out
       | of ice for weekend gatherings with this trick.
        
       | JeremyNT wrote:
       | There was a short-lived show called "Going Deep With David Rees"
       | where the host explores this in a humorous manner.
       | 
       | It's S1E1, I believe it is available on Amazon. You might be able
       | to find excerpts on youtube.
        
       | keith wrote:
       | I've gotten excellent results using an aquarium pump in a cooler.
       | Essentially making a tiny Clinebell ice maker in your freezer. If
       | you position it right and use the right amount of power, you get
       | zero cloudiness at any point in the block. Best sample I was able
       | to make (the second slide is more impressive, not sure why I
       | didn't post that first):
       | https://www.instagram.com/p/BfRgI71B1h7/?hl=en
       | 
       | Major hassle though. And is the aquarium pump food safe? Probably
       | better to go with the directional freezing method.
       | 
       | Regardless, I'm pretty sure Camper English mentions this
       | somewhere in his archives - he's tried every single method as far
       | as I can tell. He is the godfather of clear ice.
        
       | ir77 wrote:
       | is it me or pretty much all of those icecubes are infested with
       | air bubbles?
       | 
       | i'd think the "cocktail ice" criteria would be to be 100% clear.
       | I make my own ice, usually in the winter, because it's fun when
       | it's -20 outside and i stock pile it in a deep freezer for the
       | remainder of the year.
       | 
       | process: + fill a small cooler almost to the top with water +
       | leave the lid open and leave the cooler outside over night, or 2
       | nights, depends on the size + *key*: you want to remove the ice
       | from the cooler before it freezes all the way through, ideally
       | you want ~2 inches of water left on the bottom unfrozen. ice
       | freezes from top to bottom, so all the air and impurities keep
       | getting pushed down. this top layer will pretty much be perfect,
       | you may have to wash off the top layer due to frost/snow that
       | have accumulated over night. +. take your new slap of ice and
       | score it with a bread cutting serrated knife, tap the knife with
       | a wooden spoon and you'll have a perfect cut of a of a huge chuck
       | of ice. keep serrating/hitting into smaller chunks.
        
         | schwartzworld wrote:
         | Boiling water before freezing is another way of removing
         | dissolved gases.
        
           | brenns10 wrote:
           | Tested on this very website!
           | 
           | https://www.alcademics.com/2017/10/boiled-versus-rested-
           | wate...
           | 
           | Conclusion they came to (your opinion may vary) is that it's
           | not worth the time and energy to get e.g. 1/2" more clear
           | ice.
        
         | KevinGlass wrote:
         | The author of the website not only describes this exact method
         | but he also invented the method.
         | 
         | If you scroll to the bottom of this page you can see an example
         | of perfect clear, if not smoothed, ice:
         | 
         | https://www.alcademics.com/2017/05/how-to-monogram-your-ice-...
        
       | dr_dshiv wrote:
       | > Hello! If you're heard of directional freezing, learned to make
       | clear ice in a cooler or in a thermos, or purchased clear ice
       | cube trays, that information all came from me, Camper English,
       | writing here on Alcademics.
       | 
       | > My big discovery of what became known as directional freezing
       | was in 2009, and now it's used all over the world in smaller
       | cocktail bars, in homes, and in the form of many commercial ice
       | cube trays (none of which are owned by me, sadly).
       | 
       | Interesting...
        
       | ReptileMan wrote:
       | Anyone being successful with some diy Peltier or compressor
       | solution to make big blocks?
       | 
       | I need big blocks, more than my freezer can cope, but not enough
       | to justify couple of thousand EUR worth of machine.
        
         | jrockway wrote:
         | > I need big blocks
         | 
         | I did some searching and at least in my neck of the woods it
         | seems that such blocks can be ordered and delivered. Maybe you
         | don't need to DIY and you can just buy what you need?
        
         | dr_orpheus wrote:
         | Can you justify a few hundred for a big chest freezer and a
         | cooler? Then you can use the cooler method described in this
         | link or in one of the other comments from ir77 on this thread.
         | But just put the cooler inside the big chest freezer.
         | 
         | https://www.alcademics.com/2010/08/a-homemade-giant-crystal-...
        
           | ReptileMan wrote:
           | It is also terribly slow. I was thinking about something like
           | a cold plate on top of which there is pot of water with
           | insulated sides that freezes from the bottom up - and
           | something to move the water around. so you get constant
           | remelt of the top layer so no impurities.
           | 
           | A second hand ice cream maker could provide the cooling
           | power.
        
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