[HN Gopher] Knots smaller than human hair make materials unusual...
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       Knots smaller than human hair make materials unusually tough
        
       Author : gmays
       Score  : 116 points
       Date   : 2023-03-11 14:20 UTC (2 days ago)
        
 (HTM) web link (www.caltech.edu)
 (TXT) w3m dump (www.caltech.edu)
        
       | thriftwy wrote:
       | I wonder if it is possible to drive multiple carbon nanotubes
       | through C60 buckyballs to create a fabric which has tensile
       | strength of C-C binding.
        
       | siliconunit wrote:
       | Interesting behaviour, usually any normal rope knot makes the
       | rope weaker at the point of maximum curvature/choking etc. Would
       | be enlightening to get a comparison why the different behaviours,
       | just a scale/friction non linearities?
        
         | mihaaly wrote:
         | They claim the structure is tougher (absorbs more energy) not
         | stronger (maximum force before breaks). As far as I see they
         | say nothing about if it is stronger or weaker than straight
         | lines. Likely because it is weaker due to the curvatures
         | leading to stress peaks in the material before the ultimate
         | force of two straight filaments was reached. They should have
         | presented the force-displacement diagram too which is essential
         | data (maybe the original article has it). I'd be curious seeing
         | the force-displacement diagram of the two illustrated
         | experiment compared to the diagram of two straight fibres
         | tested.
         | 
         | Also I guess the toughness is just a relative matter to the
         | dimensions of the structure but since uses much more material
         | than two straigh fibres it is less tough by weight (due to the
         | decreased strength). If the same amount of material was
         | connecting the top and bottom with straight lines then that
         | would lead to the toughest situation of all (absorbing the most
         | energy). Again, guessing.
         | 
         | In the video the woven material may have tighter threads with
         | stronger friction or more uneven friction distribution leading
         | to reaching the yield limit of the filaments quicker. The woven
         | with some 'lubrication' should have had similar properties
         | assuming the same amount (length or weight) of material
         | included. I'd also be curious then about the reproducibility of
         | the results on the same kind of structure. Like if making the
         | same knotted pattern would lead to the same results or slight
         | deviation of geometry was affecting the end results
         | significantly.
        
         | cwillu wrote:
         | It looks like the loop of the knot permits slack which in turn
         | causes stress on the fiber to be taken up by straining
         | neighbouring weaves, rather than causing the stressed fiber to
         | immediately strain to its failure point.
        
       | lapinot wrote:
       | Not sure "knot" is the best wording. This looks like knitting. It
       | is well known that knitted material is very strong and very
       | flexible (much more elastic than weaving). And that all of
       | knitting/weaving/braiding already enable to improve properties
       | from initial material. Not so sure how the scale is relevant. I
       | guess the contribution from the paper is that this is in the
       | context of 3d printing.
        
       | A_D_E_P_T wrote:
       | > The knots were not tied but rather manufactured in a knotted
       | state by using advanced high-resolution 3D lithography capable of
       | producing structures in the nanoscale.
       | 
       | This would be difficult to scale. And it's possible, even likely,
       | that it can't be applied to existing strong fibers, which are
       | drawn at very low diameters. The paper does its best to bury the
       | lede, but the polymer they were using was acrylic-based, and
       | likely very weak in comparison with, e.g., Dyneema or aramid
       | fibers.
       | 
       | There are quite a lot of papers which examine the mechanical
       | properties of nano-lattice and nano-architected materials, made
       | with lithographic techniques, but I think that the commercial
       | viability of these materials is effectively zero. And, in many
       | cases, as here, it's not clear that they'd be superior to the
       | standard high-strength materials that are already so ubiquitous.
        
         | nick123567 wrote:
         | Why would lithography not scale? We've got plenty of mass
         | production lithography with microchips.
        
           | thfuran wrote:
           | Older processes are cheaper, but 5nm node costs something
           | like $25,000 per square foot (with around 0.1 defects per
           | square cm, which may result in waste) and doesn't do pieces
           | larger than about 1 foot. That's pretty bad as far as
           | textiles go.
        
           | akiselev wrote:
           | Economically mass producing microchips is only possible
           | because they are 100s of square millimeters in size and very
           | valuable per square mm. Any bigger than that and error rates
           | in the fab process start to destroy the yield.
           | 
           | These fibers are used in much bigger applications like body
           | armor or mechanical composite parts where the surface area is
           | on the order of square meters, not millimeters.
        
             | AlotOfReading wrote:
             | Modern panel fabs use fine masking over like 10sq. meters
             | with precision on the same order of this (~dozens of
             | micrometers), and people have successfully shown
             | lithography over similar panel sizes by separate exposures.
        
             | HPsquared wrote:
             | The feature size is a LOT bigger than microchips though:
             | 
             | "Each knot is around 70 micrometers in height and width,
             | and each fiber has a radius of around 1.7 micrometers"
             | 
             | That is, cheaper lithography methods could presumably be
             | used.
        
         | bigfatfrock wrote:
         | I'm shocked daily by HN comment depth, what a breadth of
         | experience people have. Thanks for the insight.
        
           | nh23423fefe wrote:
           | This place is all culture. People are smart and varied
           | everywhere. But here we try to enforce a culture is that
           | assigns low status to low effort trash. It doesn't always
           | work. But that's the expectation, I don't think anything else
           | could work. Comments should be for the community not to
           | spread low information barnacles on every piece of original
           | thought.
        
             | ant6n wrote:
             | This place also suffers from the Dunning-Kruger-Effekt.
        
               | FieryTransition wrote:
               | I guess you could argue, that most places suffer from
               | that, as everyone has a boundary, at which they don't
               | understand things. But the effect itself, is probably
               | more relevant in an organization, as it was used to
               | describe management.
        
           | daniel_reetz wrote:
           | I want to offer a tempered view. The comment does seem deep
           | and it probably is. But I work in physical prototyping - new
           | products, new technologies. I do the "design and manufacture
           | from real materials in the real world" part. I own a few
           | hundred thousand dollars in advanced machinery and make parts
           | for FAANGs and tiny research startups. I'm a named inventor
           | on something like 16 patents. And yet daily, I read
           | confident, well worded answers here -- about my domain --
           | which reflect views completely divorced from reality, or in
           | living in some strange parallel reality.
           | 
           | Personally, I try to recognize this as an opportunity for me
           | to be humble (as I never know who may read my comments from a
           | higher place of skill and domain knowledge), and also to take
           | what is posted here with a grain of salt.
        
         | dahfizz wrote:
         | I don't see a reason why the lithography method is necessary
         | here. One could design a manufacturing process which ties the
         | knots mechanically, just like woven fabrics.
         | 
         | Caltech probably already has the lithography equipment and
         | expertise on hand, so they did it that way. They aren't trying
         | to do their research in a manufacturing-friendly way, just the
         | way that is easiest for them.
        
           | A_D_E_P_T wrote:
           | Possibly lithography was used to avoid stress concentrations
           | and kinking, which can potentially be troublesome in
           | mechanically-tied knots. (Presumably, especially at that
           | scale.)
           | 
           | With respect to knotted and woven fabrics, there's quite a
           | lot of interesting research in "3D-woven" fabrics for high-
           | impact applications like body armor. 3D fabrics are pinned by
           | fibers running through the weave top-to-bottom (Z axis) and
           | are effectively macroscopically knotted. They're also
           | commercially available:
           | 
           | https://compositeenvisions.com/product/fiberglass-e-
           | glass-3d...
           | 
           | Interesting stuff, but still very niche and not always
           | clearly superior to plain woven composite materials.
        
             | Scene_Cast2 wrote:
             | IIRC with 3D weaves, the ratio of strands to empty space
             | (that would get filled with epoxy in typical rigid part
             | applications) is significantly lower.
        
         | blacksmith_tb wrote:
         | That seems likely, though it does still seem like their results
         | might fall into the "things behave differently at micro-scale
         | and macro-scale" category. Normally we'd expect the (macro)
         | knots we're familiar with to weaken -not strengthen - the cord
         | or rope they're tied in (how much varies quite a bit with which
         | knot we're talking about, but I don't know of any that don't
         | have at least some negative impact). The little video almost
         | implies the effect is similar to stretch, that the tangled
         | version can't tighten up (with friction presumably absorbing
         | some energy) like the knotted one does.
        
         | Gravityloss wrote:
         | Anybody who's worked with cables or ropes knows they
         | spontaneously form knots quite easily. Would it be possible to
         | utilize this property in manufacturing?
         | 
         | Shake a bunch of dry fibers before applying the matrix? Are
         | they too stiff?
        
           | mjhay wrote:
           | You're more-or-less describing nonwoven fabrics, which are
           | used in a huge variety of applications. There's different
           | fabrication methods, but they are typically not as strong as
           | standard weaves since the patterning can't really be
           | controlled.
           | 
           | https://en.wikipedia.org/wiki/Nonwoven_fabric
        
           | hannasanarion wrote:
           | I believe nano-scale polymer materials composed of randomly
           | formed knots are normally just called "plastic".
        
       | bookofjoe wrote:
       | https://news.ycombinator.com/item?id=35094074
        
       | dukeofdoom wrote:
       | So if you tie a knot on a rope, and pull on both ends to breaking
       | point. Is the claim that the rope would not break at the knot.
       | Not sure how true that is.
        
         | regularfry wrote:
         | No, that is not the claim.
        
         | Out_of_Characte wrote:
         | The rope would be a series of knots. Kind of like comparing the
         | tensile strength of a scarf to synthetic wool strings (since
         | regular wool is always knotted anyway.)
        
       | nick123567 wrote:
       | The title calling this a "material" is disingenuous. One would
       | assume that they somehow tested a "bulk" material coupon even if
       | just a few mm^2. But the image in the article shows them testing
       | a single knot.
        
         | nick123567 wrote:
         | In the paper, shows a test of eight knots (two sets of four in
         | series)
        
       | BiteCode_dev wrote:
       | Maybe the pressure the knots hold is enough to maintain rows of
       | sections of the material in close enough range for the casimir
       | effect to apply, making making some part of it flexible (the
       | material) and some part of it super resistant (the quantum
       | fluctuation zone) which ends up giving this property.
        
         | t344344 wrote:
         | Way too big for quantum stuff, it is just plain friction.
        
           | BiteCode_dev wrote:
           | Most probably, but throwing geckos at knots is more fun.
        
             | bglazer wrote:
             | The adhesion of the gecko's foot is caused by van der waals
             | forces, not the Casimir effect, just fyi
        
               | BiteCode_dev wrote:
               | Thank you for correcting me.
        
             | bqmjjx0kac wrote:
             | It won't pass the IRB if you describe it like that.
        
       | itronitron wrote:
       | Is anyone able to reach this site? the server seems to be down
        
         | boomboomsubban wrote:
         | Works fine for me, but here https://archive.is/mwRR1
        
       | harperlee wrote:
       | Coincidentally I was looking into simulating rope and knots for a
       | side project, and I don't know how to really research this other
       | than googling, does someone interested in these kinds of things
       | know? I'd like to simulate friction and tensile strenghs, and
       | other mechanical deformations (pulls, obviously).
        
         | bg46z wrote:
         | You could probably look at protein folding libraries like
         | pymol. Although not exactly the same, it's generally close
         | enough to ropes and it has enough knobs where you should be
         | able to run the simulations you want
        
           | gilleain wrote:
           | Hmmm. PyMol is molecular viewer, which has a python scripting
           | interface to various libraries ... but is not a folding
           | library I would say.
           | 
           | There is some research into the topology of DNA (especially
           | circular DNA, like plasmids which is a knot) that considers
           | things like writhe and twist. Not sure it would adapt too
           | well to macroscopic systems though.
           | 
           | There is also the excellent KnotPlot for actually drawing the
           | knots. I bought a licence once on a whim, but rarely use it
           | :)
        
         | AlotOfReading wrote:
         | In general, the interesting properties of real ropes are not
         | well-modeled by simulation. Dirt, abrasion, water, stress
         | concentrations, and other real factors will dramatically impact
         | the results you get out in the real world. That's why these
         | things are experimentally verified and ropes used in safety-
         | critical applications (are supposed to) have huge safety
         | margins, regular monitoring, and ideally regular replacement.
         | Use the manufacturer numbers for real ropes.
         | 
         | But if you just want to simulate ropes, there's a few models
         | out there from academics going "let's try and model this
         | difficult system more accurately". Take a look at stuff like
         | imc-der [0] and ridgerunner [1].
         | 
         | [0] https://github.com/QuantuMope/imc-der
         | 
         | [1] https://jasoncantarella.com/wordpress/software/ridgerunner/
        
         | GistNoesis wrote:
         | Maybe you can look into (extended) position based dynamics
         | https://positionbaseddynamics.readthedocs.io/en/latest/about...
         | for ropes.
         | 
         | If knots are what's interest you more, then maybe you can have
         | a look at the self-collision avoidance of "Repulsive Curves"
         | http://www.cs.cmu.edu/~kmcrane/Projects/RepulsiveCurves/
        
       | eimrine wrote:
       | I know from fishing that if you have a spontaneous tie/knot on
       | your 0,2mm line than it is dead but 0.4mm is almost always able
       | to be unknot.
        
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       (page generated 2023-03-13 23:01 UTC)