[HN Gopher] Home-Built Scanning Tunneling Microscope
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       Home-Built Scanning Tunneling Microscope
        
       Author : _Microft
       Score  : 265 points
       Date   : 2021-04-08 16:45 UTC (6 hours ago)
        
 (HTM) web link (dberard.com)
 (TXT) w3m dump (dberard.com)
        
       | leblancfg wrote:
       | Can we add [2015] to the title?
        
       | prennert wrote:
       | His day-job is pretty mind-blowing, too. He basically works on
       | combing DNA, by squashing it "into nanogrooves [that] are less
       | than 50 nm"
       | 
       | https://dberard.com/research/
       | 
       | edit: added description of his work
        
         | feralimal wrote:
         | Yes, look at all that squashed DNA, lol.
         | 
         | Seriously though, how do we know that is DNA? It just looks
         | like wiggly worms.
         | 
         | And the DNA pic is black and white, but the picture of graphite
         | is in colour. How is it in colour? Is it 'enhanced' with
         | photoshop or something?
        
           | amelius wrote:
           | DNA extraction is a routine procedure used to isolate DNA
           | from the nucleus of cells.
           | 
           | More here:
           | https://www.sciencelearn.org.nz/resources/2036-dna-
           | extractio...
        
           | adge wrote:
           | You can't actually "see" DNA itself because it is smaller
           | than the wavelength of light. Those groves are 50nm and the
           | wavelength of blue light is about 480nm.
           | 
           | So how then are the images generated?
           | 
           | It uses a technique called Fluorescence Microscopy:
           | https://en.wikipedia.org/wiki/Fluorescence_microscope
           | 
           | You essentially stick some special molecules on the DNA that
           | absorb light in one frequency and then they emit light in
           | another frequency. So you blast the molecules with light of
           | one frequency and then use a dichroic mirror to filter that
           | light out and you only see the emissions and thus you see
           | where the DNA is, but you don't "see" the DNA itself.
           | 
           | Like STM itself what we mean when we "see" something at those
           | length scales is interesting. Scanning Tunnelling Microscopy
           | is like a blind man reading braille - not really "seeing"
           | anything but getting enough info to describe the picture.
           | 
           | source: I used to work in the same lab as Dan. Hi Dan!
        
             | feralimal2 wrote:
             | This is a useful explanation - thanks!
             | 
             | What does this mean to the value of what we are "seeing"?
             | 
             | The example used before - that it is equivalent to a deaf
             | man seeing a music visualisation - is apt. It is some sort
             | of model, but not particularly close. It might still be
             | useful, of course.
        
           | snalty wrote:
           | False colour is pretty much standard for many imaging
           | techniques including STM.
        
             | s0rce wrote:
             | Its not even really false color, its just a look up table
             | applied to the data, which is some equi-tunneling current
             | or height map, don't know exactly how this is done, bit out
             | of my field.
        
               | jacquesm wrote:
               | The tip is pointing down, so an increase in current would
               | indicate a decrease in 'Z' coordinate of the sample
               | surface.
        
       | ahartmetz wrote:
       | I worked with a simple STM in a lab exercise. At the beginning,
       | we created a new, clean tip. Guess how we did that?...
       | 
       | We cut a piece of ordinary steel wire diagonally with an ordinary
       | wire cutter. Somehow we did it right - the first one worked. It
       | was all somewhat fiddly and sometimes the image was noisy. But we
       | did get images of atoms.
        
       | jacquesm wrote:
       | I think I'm going to build this with my kids. What better way to
       | show them atoms than to actually make them build a microscope
       | that shows you the things directly?
        
         | biswaroop wrote:
         | This is a wonderful idea. Children (and adults) learn best by
         | doing. There's such a big difference between watching some tv
         | show and making an actual experiment to see structures
         | invisible to the naked eye. I know I would have been psyched to
         | see atoms as a kid.
        
         | feralimal wrote:
         | I'm sure its a cool project.
         | 
         | But its not showing things directly, is it? Its interpreting a
         | frequency and converting that to an image. Is it really that
         | different to a music visualiser?
        
           | crispyambulance wrote:
           | > But its not showing things directly, is it?
           | 
           | I don't understand the downvotes. That's an honest
           | fundamental question.
           | 
           | It's not "showing things directly" because it can't. The
           | limit of what you can see with light is proportional to the
           | wavelength of the light (this is called the diffraction
           | limit). For visible light and lens-based optics that's around
           | 1/2 micron.
           | 
           | The distance between the atoms in that graphite is ~3
           | angstroms, that about 2000 times smaller than the diffraction
           | limit for visible light.
           | 
           | You CAN get atomic resolution with a transmission electron
           | microscope. Instead of light it uses electrons and has a far
           | finer diffraction limit that visible light. Instead of lenses
           | it uses electrostatic deflection.
        
             | jacquesm wrote:
             | > I don't understand the downvotes.
             | 
             | Because the comment is factually wrong. Because it tries to
             | argue something in bad faith.
             | 
             | > That's an honest fundamental question.
             | 
             | But it wasn't a question, it was a statement, and a faulty
             | one at that.
             | 
             | Best case interpretation would require substituting
             | 'current' for 'frequency' and even then it would be
             | inaccurate because the current is a proxy for the
             | Z-distance to the tip which is then used to convert to a 3D
             | map, which in turn can be visualized.
             | 
             | It is fairly obvious that this is an indirect process so
             | clear the word 'directly' wasn't about 'seeing atoms' but
             | all about the fact that you can make the observations
             | yourself.
             | 
             | Whether you are measuring a current or looking through an
             | eyepiece both are observations. And looking at the
             | resulting image is _also_ an observation.
             | 
             | As opposed to reading about STMs and looking at pretty
             | pictures online or in books.
             | 
             | It's a shallow comment masquerading as an insightful one,
             | the worst way to derail any conversation.
        
               | feralimal2 wrote:
               | The reason for the downvotes.... won't be popular to
               | hear, but here it is.
               | 
               | This forum apparently values the scientific outlook,
               | which is purported to be a skeptical one. Do not commit
               | to accepting whatever-it-is without evidence, right?
               | 
               | But that unpopular, question opinions are so downvoted
               | (which has the effect that replies cannot be posted until
               | the next day when no one is watching) speaks volumes
               | about how skeptical people really are. How much
               | application of the scientific method do people actually
               | use in their lives?
               | 
               | What we really have in science, and society in general,
               | is an echo chamber where lots of lip service is given to
               | the scientific method but no one actually implements it
               | personally. Then when someone like me comes along and
               | critically reviews the presentation, it leaves people
               | feeling uncomfortable as they realise just how much they
               | have taken on trust.
               | 
               | So, the answer is to downvote. Its not pretty but
               | everyone can get back into the comfortable echo chamber.
               | And in preventing unpopular skeptical opinions (ie
               | maintaining the echo chamber) is what HN is here to
               | facilitate.
        
               | [deleted]
        
               | argvargc wrote:
               | The GP's "statement" contained three relevant sentences,
               | two ending with question-marks. I learned from both your
               | answer and its parent, furthering conversation, for me at
               | least.
        
           | jacquesm wrote:
           | Directly as in: you do it yourself, without going through a
           | bunch of intermediaries who will dazzle you with their pretty
           | pictures, you yourself are the one observing the results.
           | 
           | Of course a STM does not work with visible light so it's
           | pretty damn obvious that any measurements will use some other
           | mechanism, and will have to have their measurements converted
           | into an image that we can see. But that does not mean we are
           | not observing. As opposed to reading about someone else's
           | observations.
           | 
           | I take it you also believe that quasars have not been
           | observed and ditto for the dark side of the moon?
        
           | minitoar wrote:
           | I mean, what is your brain doing if not that?
        
             | feralimal wrote:
             | You don't think there's a difference between what you see
             | with your naked eye, and what is visualised for you by
             | sensors and software?
        
               | gryn wrote:
               | do you think your eye is not a sensor ?
        
               | feralimal wrote:
               | Of course your eye is a sensor. As are all your senses.
               | The difference is that the input it receives is
               | unmediated by external sensors and software. Visualising
               | atoms or DNA is fine, but it is an inferior source of
               | information. By a long way.
               | 
               | Imagine you were born deaf and couldn't hear music. But
               | that someone showed you a music visualiser.
               | 
               | Do you think if you were watching the output of that
               | visualiser you would now know the music in some
               | meaningful way?
        
               | jacquesm wrote:
               | Would it be possible for you to try at least to
               | contribute to the discussion? This out of hand dismissal
               | seems to be a bit of an issue for you, maybe try harder?
               | 
               | https://news.ycombinator.com/item?id=26743591
        
               | nightfly wrote:
               | Sure, but digital cameras are still useful.
        
           | s0rce wrote:
           | Its a 2D map of the tip position which is a function of the
           | tunneling current over a surface. Its not frequency.
        
         | [deleted]
        
       | edge17 wrote:
       | Can someone ELI5 the vibration isolation [0] part of it? I kind
       | of get what he's doing, but would appreciate some analogy if it
       | makes sense to make an analogy.
       | 
       | [0] https://dberard.com/home-built-stm/vibration-isolation/
        
         | jacquesm wrote:
         | In a nutshell: the vibrations that affect the imaging are
         | pretty high frequency. So to get rid of them he has isolated
         | his whole setup in such a way that if there is a vibration it
         | will be _well_ under the lower cut-off frequency that is part
         | of the measurements. So the whole apparatus may go up or down
         | but that won 't affect the measurements. If the whole thing
         | would not be isolated then the rumble from the tires of a
         | passing car or a jet flying over would utterly ruin the
         | measurements.
         | 
         | Especially the vibration damping is nicely done, it is zero
         | contact and has the effect of stopping any beginning
         | oscillation in its tracks.
        
         | terofle wrote:
         | Imagine painting with a paintbrush while standing on a jumping
         | castle with 5 jumping children.
         | 
         | If you have no vibration isolation, it is nearly impossible to
         | draw a very thin and straight line.
         | 
         | (Maybe a bit exaggerated, the vibration analogy is a bit weaker
         | in reality)
        
         | sleavey wrote:
         | Incidentally all of the techniques listed there are used for
         | suspensions in LIGO, Virgo and other ground-based gravitational
         | wave detectors, where the problem is the same: stop seismic
         | noise from moving the object under test.
        
       | kurthr wrote:
       | CA3140 OpAmps also work well.
       | 
       | The comments about 1pF feedback do speak to one of the challenges
       | with feedback stability, where stray capacitance on the proto-
       | board may or may not be present.
        
         | analog31 wrote:
         | Indeed, a 100-Meg feedback resistor is mostly a capacitor. You
         | could think of it as an integrator with DC bias control. This
         | is probably the best article I've seen about transimpedance
         | amplifiers:
         | 
         | https://electrooptical.net/static/oldsite/www/frontends/fron...
        
           | jacquesm wrote:
           | You could draw a pretty interesting graph of how the
           | resistance/parasitic capacitance relationship governs which
           | component is dominant at the high end of the resistance
           | range.
        
       | amelius wrote:
       | Can you image non-conductive surfaces with this technique?
        
         | ortusdux wrote:
         | Best you can do is gold plate the object you would like to
         | scan. Sputter coating is the preferred method.
         | 
         | https://en.wikipedia.org/wiki/Scanning_electron_microscope#S...
        
           | oasisbob wrote:
           | That's for SEM. I've never heard of sputter coating used for
           | STM.
        
             | ortusdux wrote:
             | You are right, I got those two methods mixed up. It looks
             | like gold sputter coating would be a good solution for the
             | home made tungsten STM tips mentioned in the link.
        
           | Retric wrote:
           | That's a SEM which is significantly lower resolution, but
           | lets you zoom in and out across a huge range.
           | 
           | STM on the other hand is for looking at individual atoms so
           | coating a surface is just going to show that coating.
           | https://en.wikipedia.org/wiki/Scanning_tunneling_microscope
        
         | oasisbob wrote:
         | Sort of?
         | 
         | STM is frequently used to characterize adsorbed molecular
         | monolayers on a graphite substrate.
         | 
         | You're obviously depending on electron conduction to image the
         | sample, but you can image all sorts of things which wouldn't be
         | considered conductive as a bulk material.
        
         | smitty1110 wrote:
         | Nope, the technique for that is an Atomic Force Microscopy[1].
         | 
         | 1: https://en.wikipedia.org/wiki/Atomic_force_microscopy
        
           | alted wrote:
           | And it turns out DIY atomic force microscopes are possible
           | too! (e.g., [1]) It's probably less likely to get all the way
           | to atomic resolution (0.01nm) like a scanning tunneling
           | microscope, but atomic force microscopes can take many types
           | of 1-to-1000nm-scale measurements and are often more
           | practically useful.
           | 
           | [1] https://hackaday.com/2014/04/29/a-diy-atomic-force-
           | microscop...
        
           | waiquoo wrote:
           | OR helium ion microscopy, but that is not as widely available
           | afaik
           | 
           | 1:
           | https://en.wikipedia.org/wiki/Scanning_helium_ion_microscope
        
       | fit2rule wrote:
       | This is an amazing project, in so many ways.
       | 
       | My first thought is, the implant business has now got a problem.
       | Soon enough, anyone and their pal will be able, finally, to
       | validate their silicon at adequate scale.
        
       | terofle wrote:
       | This project is great.
       | 
       | Last semester at university lab, our group tried to rebuild it in
       | our lab.
       | 
       | Through our spectacular fail, we learned how amazing this project
       | actually is. It is harder than it seems.
       | 
       | One can learn very much about piezo electronics, especially about
       | OPamp circuits. And do not underrate the damping!
        
         | jacquesm wrote:
         | And the amplification circuitry, that's not trivial. I was
         | actually surprised he got away with having the wiring out in
         | the open without shielding it for EMI.
        
           | FuriouslyAdrift wrote:
           | In the section for "Electronics" is this line "I place a
           | metal can over the STM during scanning to shield the tip and
           | preamp. Without the shield, the images produced by the STM
           | are dominated by 60 Hz noise pickup."
        
             | jacquesm wrote:
             | Ah! I totally missed that, thank you. I thought the
             | pictures were of the scanner in operation, and that detail
             | really confused me.
        
       | lappa wrote:
       | Similar project: http://e-basteln.de/other/stm/overview/
        
       | dang wrote:
       | Small past threads:
       | 
       |  _Home Built Scanning Tunneling Microscope Electronics_ -
       | https://news.ycombinator.com/item?id=9752215 - June 2015 (9
       | comments)
       | 
       |  _Home-Built Scanning Tunneling Microscope_ -
       | https://news.ycombinator.com/item?id=8884085 - Jan 2015 (1
       | comment)
        
       | twobitshifter wrote:
       | Ben Krasnow built his electron scanning microscope back in 2011.
       | I never expected to see that one upped.
       | https://benkrasnow.blogspot.com/2011/03/diy-scanning-electro...
        
         | _Microft wrote:
         | The scanning electron microscope project seems far more
         | involved than this one. I submitted the SEM before this one by
         | the way but it unfortunately did not catch on.
        
         | oasisbob wrote:
         | Homebrew STM is a pretty common and simple in principle. I used
         | to have a chemistry prof who would guide a group of high
         | schoolers through building an STM head each year.
         | 
         | Homebrew SEM is probably much more difficult and rare.
        
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