| II.— | Aniline black | 1/2 ounce |
|---|---|---|
| Pure alcohol | 15 ounces | |
| Concentrated glycerine | 15 ounces |
Dissolve the aniline black in the alcohol, and add the glycerine. Ink as before. The aniline inks containing glycerine are copying inks.
| III.— | Alcohol | 2 ounces |
|---|---|---|
| Aniline color | 1/4 ounce | |
| Water | 2 ounces | |
| Glycerine | 4 ounces |
Dissolve the aniline in the alcohol and add the water and glycerine.
| IV.— | Castor oil | 2 ounces |
|---|---|---|
| Cassia oil | 1/2 ounce | |
| Carbolic acid | 1/2 ounce |
Warm them together and add 1 ounce of aniline color. Indelible typewriter inks may be made by using lampblack in place of the aniline, mixing it with soft petrolatum and dissolving the cooled mass in a mixture of equal parts of benzine and turpentine.
Red.—
| I.— | Bordeaux red, O. S. | 15 parts |
|---|---|---|
| Aniline red, O. S. | 15 parts | |
| Crude oleic acid | 45 parts | |
| Castor oil enough to make | 1,000 parts |
Rub the colors up with the oleic acid, add the oil, warming the whole to 100° to 110° F. (not higher), under constant stirring. If the color is not sufficiently intense for your purposes, rub up a trifle more of it with oleic acid, and add it to the ink. By a little experimentation you can get an ink exactly to your desire in the matter.
Blue-Black.—
| II.— | Aniline black, O. S. | 5 parts |
|---|---|---|
| Oleic acid, crude | 5 parts | |
| Castor oil, quantity sufficient to | 100 parts. |
Violet.—
| III.— | Aniline violet, O. S. | 3 parts |
|---|---|---|
| Crude oleic acid | 5 parts | |
| Castor oil, quantity sufficient to | 100 parts. |
The penetration of the ink may be increased ad libitum by the addition of a few drops of absolute alcohol, or, better, of benzol.
The common writing fluids depend mostly upon galls, logwood, or aniline for coloring. There are literally thousands of formulas. A few of the most reliable have been gathered together here:
I.—Aleppo galls (well bruised), 4 ounces; clean soft water, I quart; macerate in a clean corked bottle for 10 days or a fortnight or longer, with frequent agitation; then add of gum arabic (dissolved in a wineglassful of water), 1 1/2 ounces; lump sugar, 1/2 ounce. Mix well, and afterwards further add of sulphate of iron (green copperas crushed small), 1 1/2 ounces. Agitate occasionally for 2 or 3 days, when the ink may be decanted for use, but is better if the whole is left to digest together for 2 or 3 weeks. When time is an object, the whole of the ingredients may at once be put into a bottle, and the latter agitated daily until the ink is made; and boiling water instead of cold water may be employed. Product, 1 quart of excellent ink, writing pale at first, but soon turning intensely black.
II.—Aleppo galls (bruised), 12 pounds; soft water, 6 gallons. Boil in a copper vessel for 1 hour, adding more water to make up for the portion lost by evaporation; strain, and again boil the galls with water, 4 gallons, for 1/2 hour; strain off the liquor, and boil a third time with water, 2 1/2 gallons, and strain. Mix the several liquors, and while still hot add of green copperas (coarsely powdered), 4 1/2 pounds; gum arabic (bruised small), 4 pounds. Agitate until dissolved, and after defecation strain through a hair sieve, and keep in a bunged cask for use. Product, 12 gallons.
III.—Aleppo galls (bruised), 14 pounds; gum, 5 pounds. Put them in a small cask, and add boiling soft water, 15 gallons. Allow the whole to macerate, with frequent agitation, for a fortnight, then further add of green copperas, 5 pounds, dissolved in water, 7 pints. Again mix well, and agitate the whole once daily for 2 or 3 weeks. Product, 15 gallons.
II.—A strong decoction of logwood, with a very little bichromate of potash.
II.—Bruised galls, 14 pounds; gum, 5 pounds. Put them in a small cask, and add of boiling water, 15 gallons. Allow the whole to macerate, with frequent agitation, for 2 weeks, then further add green copperas, 5 pounds, dissolved in 7 pints water. Again mix well, and agitate the whole daily for 2 or 3 weeks.
NOTE.—No gum or sugar is proper and on no account must the acid be omitted. When intended for copying, 5 1/2 ounces of galls is the quantity. On the large scale this fine ink is made by percolation.
This is usually prepared by adding a little sugar to ordinary black ink, which for this purpose should be very rich in color, and preferably made galls prepared by heat. Writing executed with this ink may be copied within the space of 5 or 6 hours, by passing it through a copying press in contact with thin, unsized paper, slightly damped, enclosed between 2 sheets of thick oiled or waxed paper, when a reversed transcript will be obtained, which will read in proper order when the back of the copy is turned upwards. In the absence of a press a copy may be taken, when the ink is good and the writing very recent, by rolling the sheets, duly arranged on a ruler, over the surface of a flat, smooth table, employing as much force as possible, and avoiding any slipping or crumbling of the paper. Another method is to pass a warm flatiron over the paper laid upon the writing. The following proportions are employed:
I.—Sugar candy or lump sugar, 1 ounce; or molasses or moist sugar, 1 1/4 ounces; rich black ink, 1 1/2 pints; dissolve.
II.—Malt wort, 1 pint; evaporate it to the consistence of a syrup, and then dissolve it in good black ink, 1 1/4 pints.
III.—Solazza juice, 2 ounces; mild ale, 1/2 pint; dissolve, strain, and triturate with lampblack (previously heated to dull redness in a covered vessel), 1/4 ounce; when the mixture is complete, add of strong black, 1 1/2 pints; mix well, and in 2 or 3 hours decant the clear.
After making the above mixtures, they must be tried with a common steel pen, and if they do not flow freely, some more unprepared ink should be added until they are found to do so.
| Gum arabic | 1.5 parts |
| Sugar | 7.5 parts |
| Sulphuric acid, 66° B | 10.5 parts |
| Aniline blue | 1.5 parts |
| Carbolic acid | 0.5 parts |
| Mirobalan extract to make | 1,000 parts. |
This ink when first used has a bluish tint, afterwards becoming black.
| Iron sulphate | 30 parts |
| Copper sulphate | 0.5 parts |
| Sulphuric acid | 2 parts |
| Sugar | 8 parts |
| Wood vinegar, rectified | 50 parts |
| Indigo carmine | 30 parts |
Reduce by evaporation 10 volumes of any good ink to 6, then add 4 volumes of glycerine. Or manufacture some ink of nearly double strength, and add to any quantity of it nearly an equal volume of glycerine.
| Aniline green (soluble) | 2 parts |
| Glycerine | 16 parts |
| Alcohol | 112 parts |
| Mucilage of gum arabic | 4 parts |
Dissolve the aniline in the alcohol, and add the other ingredients. Most of the gum arabic precipitates, but according to the author of the formula (Nelson) it has the effect of rendering the ink slow-flowing enough to write with. Filter. {416}
II.—Blue.—Resorcin blue M, 10 parts.
Dissolve by means of heat in a mixture of:
| Dilute acetic acid | 1 part |
| Distilled water | 85 parts |
| Glycerine | 4 parts |
| Alcohol, 90 per cent | 10 parts |
III.—Green.—Aniline green, water solution, 15 parts; glycerine, 10 parts; Water, 50 parts; alcohol, 10 parts.
II.—Red.—Take 1 part of red aniline mixed with 10 parts of acetic acid; 5 parts of citric acid, and 25 parts of mucilage, all well mixed. For use, mix 1 part of the paste with 16 parts of water.
III.—Blue.—Take 2 parts of aniline blue mixed with 10 parts of acetic acid; 5 parts of citric acid, and 40 parts of mucilage, all well mixed. For use, mix 1 part of the paste with 8 parts of water.
IV.—Violet.—Use the same ingredients in the same proportions as blue, with the difference that violet aniline is used instead of blue aniline.
V.—Green.—Take 1 part of aniline blue; 3 parts of picric acid, mixed with 10 parts of acetic acid; 3 parts of citric acid, and 80 parts of mucilage. For use, 1 part of this paste is mixed with 8 parts of water.
VI.—Copying.—Take 6 parts of pulverized bichromate of potash, mixed with 10 parts of acetic acid and 240 parts of liquid extract of logwood, and add a pulverized mixture of 35 parts of alum, 20 parts of sal sorrel, and 20 parts mucilage. Mix well. For use, 1 part of this paste is mixed with 4 parts of hot water.
II. (Normandy).—To 12 pounds of Campeachy wood add as many gallons of boiling water. Pour the solution through a funnel with a strainer made of coarse flannel, or 1 pound of hydrate, or acetate of deutoxide of copper finely powdered (having at the bottom of the funnel a piece of sponge); then add immediately 14 pounds of alum, and for every 340 gallons of liquid add 80 pounds of gum arabic or gum senegal. Let these remain for 3 or 4 days, and a beautiful purple color will be produced.
| I.— | Water-soluble nigrosin | 1 part |
|---|---|---|
| Water | 9 parts | |
| Mucilage acacia | 1 part | |
| II.— | Paris violet | 2 parts |
| Water | 6 parts | |
| Mucilage acacia | 2 parts | |
| III.— | Methyl violet | 1 part |
| Distilled water | 7 parts | |
| Mucilage acacia | 2 parts | |
| IV.— | Bordeaux red | 3 parts |
| Alcohol | 2 parts | |
| Water | 20 parts | |
| Mucilage acacia | 2 parts | |
| V.— | Rosaniline acetate | 2 parts |
| Alcohol | 1 part | |
| Water | 10 parts | |
| Mucilage acacia | 2 parts |
II.—Make as gold ink, but use silver leaf or silver bronze powder.
| III.— | Oxide of zinc | 30 grains |
|---|---|---|
| Mucilage | 1 ounce | |
| Spirit of wine | 40 drops | |
| Silver bronze | 3 drachms |
Rub together, until perfectly smooth, {417} the zinc and mucilage, then add the spirit of wine and silver bronze and make up the quantity to 2 ounces with water.
II.—Another good violet ink is made by dissolving some violet aniline in water to which some alcohol has been added. It takes very little aniline to make a large quantity of the ink.
White marks may sometimes be made on colored papers by the application of acids or alkalies. The result, of course, depends on the nature of the coloring matter in each instance, and any “ink” of this kind would be efficacious or otherwise, according to the coloring present in the paper.
II.—Boil French berries, 1/2 pound, and alum, 1 ounce, in rain water, 1 quart, for 1/2 an hour, or longer, then strain and dissolve in the hot liquor gum arabic, 1 ounce.
| Zinc white | 2 drachms |
| White precipitate | 5 grains |
| Mucilage | 1 drachm |
| Water | 6 drachms |
Triturate the zinc white with a small quantity of water till quite smooth, then add the mucilage and the remainder of the water.
INK FOR THE LAUNDRY: See Laundry Preparations.
INK FOR LEATHER FINISHERS: See Leather.
INKS FOR TYPEWRITERS: See Typewriter Ribbons.
INK FOR WRITING ON GLASS: See Etching and Glass.
See also Electro-etching, under Etching.
The process consists in engraving the design by means of the sand-blast and stencils on the surface of the article. The design or pattern is rendered conductive and upon this conductive surface a precipitate of gold, silver, platinum, etc., is applied, and fills up the hollows. Subsequently the surface is ground smooth.
| I.— | Carbolic acid | 15 grains |
|---|---|---|
| Glycerine | 2 drachms | |
| Rose water | 4 ounces | |
| II.— | Salicylic acid | 15 grains |
| Collodion | 2 1/2 drachms | |
| Spirit of ammonia | 5 1/2 drachms | |
| III.— | Fluid extract rhus toxicodendron | 1 drachm |
| Water | 8 ounces | |
| IV.— | Ipecac, in powder | 1 drachm |
| Alcohol | 1 ounce | |
| Ether | 1 ounce | |
| V.— | Betanaphthol | 30 grains |
| Camphor | 30 grains | |
| Lanolin cold cream | 1 ounce |
VI.—Spirit of sal ammoniac, whose favorable action upon fresh insect bites is universally known, is often unavailable. A simple means to alleviate the pain and swelling due to such bites, when still fresh, is cigar ashes. Place a little ashes upon the part stung, add a drop of water—in case of need beer, wine, or coffee may be used instead—and rub the resulting paste thoroughly into the skin. It is preferable to use fresh ashes of tobacco, because the recent heat offers sufficient guarantee for absolute freedom from impurities. The action of the tobacco ashes is due to the presence of {418} potassium carbonate, which, like spirit of sal ammoniac, deadens the effect of the small quantities of acid (formic acid, etc.) which have been introduced into the small wound by the biting insect.
(See also Petroleum.)
It may be stated that a dwelling, office, warehouse, or any building may be economically cleared of all pests, provided that the local conditions will permit the use of this gas. It probably would be dangerous to fumigate a building where groceries, dried fruits, meats, or prepared food materials of any kind are stored. Air containing more than 25 per cent of the gas is inflammable; therefore it would be well to put out all fire in an inclosure before fumigating. Hydrocyanic acid, in all its forms, is one of the most violent poisons known, and no neglect should attend its use. There is probably no sure remedy for its effects after it has once entered the blood of any of the higher animals. When cyanide of potassium is being used it should never be allowed to come in contact with the skin, and even a slight odor of the gas should be avoided. Should the operator have any cut or break in the skin of the hands or face it should be carefully covered with court-plaster to prevent the gas coming in contact with the flesh, or a small particle of the solid compound getting into the cut might cause death by poisoning in a few minutes’ time.
Hydrocyanic acid gas should not be used in closely built apartments with single walls between, as more or less of the gas will penetrate a brick wall. An inexperienced person should never use cyanide of potassium for any purpose, and if it be found practicable to treat buildings in general for the extermination of insects, the work should be done only under the direction of competent officials. Experiments have shown that a smaller dose and a shorter period of exposure are required to kill mice than for roaches and household insects generally, and it readily follows that the larger animals and human beings would be more quickly overcome than mice, since a smaller supply of pure air would be required to sustain life in mice, and small openings are more numerous than large ones.
The materials employed and the method of procedure are as follows: After ascertaining the cubic content of the inclosure, provide a glass or stoneware (not metal) vessel of 2 to 4 gallons capacity for each 5,000 cubic feet of space to be fumigated. Distribute the jars according to the space, and run a smooth cord from each jar to a common point near an outside door where they may all be fastened; support the cord above the jar by means of the back of a chair or other convenient object in such a position that when the load of cyanide of potassium is attached it will hang directly over the center of the jar. Next weigh out upon a piece of soft paper about 17 ounces of 98 per cent pure cyanide of potassium, using a large pair of forceps for handling the lumps; wrap up and place in a paper bag and tie to the end of the cord over the jar. After the load for each jar has been similarly provided, it is well to test the working of the cords to see that they do not catch or bind. Then remove the jar a short distance from under the load of cyanide and place in it a little more than a quart of water, to which slowly add 1 1/2 pints of commercial sulphuric acid, stirring freely. The action of the acid will bring the temperature of the combination almost to the boiling point. Replace the jars beneath the bags of cyanide, spreading a large sheet of heavy paper on the floor to catch any acid that may possibly fly over the edge of the jar when the cyanide is dropped, or as a result of the violent chemical action which follows. Close all outside openings and open up the interior of the apartment as much as possible, in order that the full strength of the gas may reach the hiding places of the insects. See that all entrances are locked or guarded on the outside to prevent persons entering; then leave the building, releasing the cords as you go. The gas will all be given off in a few minutes, and should remain in the building at least 3 hours.
When the sulphuric acid comes in contact with the cyanide of potassium the result is the formation of sulphate of potash, which remains in the jar, and the hydrocyanic acid is liberated and {419} escapes into the air. The chemical action is so violent as to cause a sputtering, and frequently particles of the acid are thrown over the sides of the jar; this may be prevented by supporting a sheet of stiff paper over the jar by means of a hole in the center, through which the cord supporting the cyanide of potassium is passed, so that when the cord is released the paper will descend with the cyanide and remain at rest on the top of the jar, but will not prevent the easy descent of the cyanide into the acid. The weight of this paper will in no way interfere with the escape of the gas.
At the end of the time required for fumigation, the windows and doors should be opened from the outside and the gas allowed to escape before anyone enters the building. A general cleaning should follow, as the insects leave their hiding places and, dying on the floors, are easily swept up and burned. The sulphate of potash remaining in the jars is poisonous and should be immediately buried and the jars themselves filled with earth or ashes. No food that has remained during fumigation should be used, and thorough ventilation should be maintained for several hours. After one of these experiments it was noted that ice water which had remained in a closed cooler had taken up the gas, and had both the odor and taste of cyanide.
For dwellings one fumigation each year would be sufficient, but for storage houses it may be necessary to make an application every 3 or 4 months to keep them entirely free from insect pests. The cost of materials for one application is about 50 cents for each 5,000 cubic feet of space to be treated. The cyanide of potassium can be purchased at about 35 cents per pound, and the commercial sulphuric acid at about 4 cents per pound. The strength of the dose may be increased and the time of exposure somewhat shortened, but this increases the cost and does not do the work so thoroughly. In no case, however, should the dose remain less than 1 hour.
The application of this method of controlling household insects and pests generally is to be found in checking the advance of great numbers of some particular insect, or in eradicating them where they have become thoroughly established. This method will be found very advantageous in clearing old buildings and ships of cockroaches.
See also Veterinary Formulas.
| I.— | Oil of cloves | 3 parts |
|---|---|---|
| Bay oil | 5 parts | |
| Eucalyptus tincture | 5 parts | |
| Alcohol | 150 parts | |
| Water | 200 parts |
II.—Tar well diluted with grease of any kind is as effective an agent as any for keeping flies from cattle. The mixture indicated has the advantage of being cheap. Applying to the legs, neck, and ears will usually be sufficient.
| Sulphur | 86 pounds |
| Extra dynamo oil | 1,000 gallons |
| By weight | ||
|---|---|---|
| I.— | Bay oil | 500 parts |
| Naphthalene | 100 parts | |
| Camphor | 60 parts | |
| Animal oil | 25 parts | |
| II.— | Bay oil, pressed | 400 parts |
| Naphthalene | 100 parts | |
| Crude carbolic acid | 10 parts | |
| Naphthalene | 4 av. ounces |
| Starch | 12 av. ounces |
Reduce to fine powder. A few grains of lampblack added will impart a light gray color, and if desirable a few drops of oil of pennyroyal or eucalyptus will disguise the naphthalene odor.
Rub into the skin of the animal and let the powder remain for a day or two, when the same can be removed by combing or giving a bath, to which some infusion of quassia or quassia chips has been added. This treatment is equally efficient for lice and ticks.
II.—Oil of eucalyptus smeared about the coop will cause the parasites to leave. To drive them out of the nests of sitting hens, place in the nest an egg that has been emptied, and into which has been inserted a bit of sponge imbibed in essence of eucalyptus. There may be used also a concentrated solution of extract of tobacco, to which phenol has been added. {420}
III.—Cover the floor or soil of the house with ground or powdered plaster, taken from old walls, etc.
A most efficacious means of getting rid of ants is spraying their resorts with petroleum. The common oil is worth more for this purpose than the refined. Two thorough sprayings usually suffice.
In armoires, dressing cases, etc., oil of turpentine should be employed. Pour it in a large plate, and let it evaporate freely. Tobacco juice is another effective agent, but both substances have the drawback of a very penetrating and disagreeable odor.
Boiling water is deadly to ants wherever it can be used (as in the garden, or yard around the house). So is carbon disulphide injected into the nests by aid of a good, big syringe. An emulsion of petroleum and water (oil, 1 part; water, 3 parts) poured on the earth has proven very efficacious, when plentifully used (say from 1 ounce to 3 ounces to the square yard). A similar mixture of calcium sulphide and water (calcium sulphide, 100 parts; water, 1,000 parts; and the white of 1 egg to every quart of water) poured into their holes is also effective.
A weak solution of corrosive sublimate is very deadly to ants. Not only does it kill them eventually, but it seems to craze them before death, so that ants of the same nest, after coming into contact with the poison, will attack each other with the greatest ferocity.
Where ants select a particular point for their incursions it is a good plan to surround it with a “fortification” of obnoxious substance. Sulphur has been used successfully in this way, and so has coal oil. The latter, however, is not a desirable agent, leaving a persistent stain and odor.
The use of carbon disulphide is recommended to destroy ants’ nests on lawns. A little of the disulphide is poured into the openings of the hills, stepping on each as it is treated to close it up. The volatile vapors of the disulphide will penetrate the chambers of the nest in every direction, and if sufficient has been used will kill not only the adult insects but the larvæ as well. A single treatment is generally sufficient.
| I.— | Water | 1 quart |
|---|---|---|
| Cape aloes | 4 ounces | |
| Boil together and add: | ||
| Camphor in small pieces | 1 1/2 ounces | |
| II.— | Powdered cloves | 1 ounce |
| Insect powder | 1 ounce | |
| Scatter around where ants infest. | ||
| III.— | Cape aloes | 1/2 pound |
| Water | 4 pints | |
Boil together and add camphor gum, 3 ounces. Sprinkle around where the ants infest.
A good bug killer is benzine, pure and simple, or mixed with a little oil of mirbane. It evaporates quickly and leaves no stain. The only trouble is the inflammability of its vapor.
The following is a popular preparation: To half a gallon of kerosene oil add a quart of spirit of turpentine and an ounce of oil of pennyroyal. This mixture is far less dangerous than benzine. The pennyroyal as well as the turpentine are not only poisonous but exceedingly distasteful to insects of all kinds. The kerosene while less quickly fatal to bugs than benzine is cheaper and safer, and when combined with the other ingredients becomes as efficient.
Where the wall paper and wood work of a room have become invaded, the usual remedy is burning sulphur. To be efficient the room must have every door, window, crevice, and crack closed. The floor should be wet in advance so as to moisten the air. A rubber tube should lead from the burning sulphur to a key-hole or auger-hole and through it, and by aid of a pair of bellows air should be blown to facilitate the combustion of the sulphur.
| I.— | Common soap | 1 av. ounce |
|---|---|---|
| Ammonium chloride | 3 av. ounces | |
| Corrosive sublimate | 3 av. ounces | |
| Water enough to make | 32 fluidounces. |
Dissolve the salts in the water and add the soap.
This will make a paste that can be painted with a brush around in the cracks and crevices. Besides, it will make an excellent filling to keep the cracks of the wall and wainscoting free from bugs of all kinds. The formula could be modified so as to permit the use {421} of Paris green or London purple, if desired. A decoction of quassia could be used to dissolve the soap. The latter paste would, of course, not be poisonous, and in many instances it would be preferred. It is possible to make a cold infusion of white hellebore of 25 per cent strength, and in 1 quart of infusion dissolve 1 ounce of common soap. The advantage of the soap paste is simply to keep the poisonous substance thoroughly distributed throughout the mass at all times. The density of the paste can be varied to suit. Kerosene oil or turpentine could replace 6 ounces or 8 ounces of the water in making the paste, and either of these would make a valuable addition.
Another paste preparation which will meet with hearty recommendation is blue ointment. This ointment, mixed with turpentine or kerosene oil, can be used to good advantage; especially so as the turpentine is so penetrating that both it and the mercury have a chance to act more effectually. It can be said that turpentine will kill the bedbug if the two come in contact; and kerosene is not far behindhand in its deadly work.